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Western Kentucky University

Surface Microstructure Evolution of Metallic Specimens Using the Large Chamber Scanning Electron Microscope

Abstract

dc:description.abstract

<p>An initial study into the use of the large chamber scanning electron microscope (LCSEM) to interrogate the surface microstructure evolution of metallic specimens has been carried out. The LC-SEM located at Western Kentucky University is the largest instrument of its type at any university in the world. As such, unique measurements can be performed due to the size of its chamber and extended view of its optic system. Strain was varied for each individual specimen, and imaged using Secondary Electrons within the gauge length as well as near the grip position. Results will show progression of surface microstructures and nickel content of metallic specimens. Additionally, results will demonstrate the capability of the LC-SEM to carry out these types of measurements. Future measurements will include the incorporation of an in-situ uniaxial load frame for dynamic studies.</p>

Degree

thesis:*
Name thesis:degree_name
Master of Science
Discipline thesis:degree_discipline
Department of Physics and Astronomy
Year
2015

Author and committee

dc:creator, dc:contributor.*
Author dc:creator
  • Egbujor, Grace
Contributors dc:contributor
  • Edward Kintzel (Director), Keith Andrew, Ivan Novikov

Subjects

dc:subject × 6

Identifiers

dc:identifier.*
Repository record dc:identifier
https://digitalcommons.wku.edu/theses/1473
OAI identifier oai:identifier
oai:digitalcommons.wku.edu:theses-2474

Chain of custody

source
Harvested from
Western Kentucky University
Base URL
digitalcommons.wku.edu/do/oai/
Last updated
2026-07-24
Source record
OAI-PMH GetRecord
citation

Egbujor, Grace. Surface Microstructure Evolution of Metallic Specimens Using the Large Chamber Scanning Electron Microscope. 2015. https://digitalcommons.wku.edu/theses/1473