An initial study into the use of the large chamber scanning electron microscope (LCSEM) to interrogate the surface microstructure evolution of metallic specimens has been carried out. The LC-SEM located at Western Kentucky University is the largest instrument of its type at any university in the world. As such, unique measurements can be performed due to the size of its chamber and extended view of its optic system. Strain was varied for each individual specimen, and imaged using Secondary Electrons within the gauge length as well as near the grip position. Results will show progression of surface microstructures and nickel content of metallic specimens. Additionally, results will demonstrate the capability of the LC-SEM to carry out these types of measurements. Future measurements will include the incorporation of an in-situ uniaxial load frame for dynamic studies.
","abstract_html":"<p>An initial study into the use of the large chamber scanning electron microscope (LCSEM) to interrogate the surface microstructure evolution of metallic specimens has been carried out. The LC-SEM located at Western Kentucky University is the largest instrument of its type at any university in the world. As such, unique measurements can be performed due to the size of its chamber and extended view of its optic system. Strain was varied for each individual specimen, and imaged using Secondary Electrons within the gauge length as well as near the grip position. Results will show progression of surface microstructures and nickel content of metallic specimens. Additionally, results will demonstrate the capability of the LC-SEM to carry out these types of measurements. Future measurements will include the incorporation of an in-situ uniaxial load frame for dynamic studies.</p>","abstract_has_math":false,"creators":["Egbujor, Grace"],"institution":null,"degree_name":"Master of Science","degree_level":null,"degree_discipline":"Department of Physics and Astronomy","degree_department":null,"school":null,"contributors":["Edward Kintzel (Director), Keith Andrew, Ivan Novikov"],"advisors":[],"committee_chairs":[],"committee_members":[],"year":2015,"date_issued":"2015-05-01T07:00:00Z","date_published":"2015-05-01T07:00:00Z","updated_at":"2026-07-24T06:08:52Z","subjects":["SEM","Microstructure","Electron","Stainless Steel","Condensed Matter Physics","Physics"],"languages":[],"rights":[],"rights_urls":[],"identifier_entries":[]},"links":{"outbound_url":"https://digitalcommons.wku.edu/theses/1473","outbound_label":"Repository record","outbound_source":"dc:identifier"},"metadata_groups":[{"id":"people","label":"People","entries":[{"key":"dc:contributor","label":"Contributor","values":["Edward Kintzel (Director), Keith Andrew, Ivan Novikov"]},{"key":"dc:creator","label":"Author","values":["Egbujor, Grace"]}]},{"id":"academic_context","label":"Academic Context","entries":[{"key":"dc:type","label":"Dc Type","values":["Thesis"]},{"key":"thesis:degree_discipline","label":"Discipline","values":["Department of Physics and Astronomy"]},{"key":"thesis:degree_name","label":"Degree Name","values":["Master of Science"]}]},{"id":"subjects_keywords","label":"Subjects and Keywords","entries":[{"key":"dc:subject","label":"Dc Subject","values":["SEM","Microstructure","Electron","Stainless Steel","Condensed Matter Physics","Physics"]}]},{"id":"identifiers","label":"Identifiers","entries":[{"key":"dc:identifier","label":"Identifier","values":["https://digitalcommons.wku.edu/theses/1473"]}]},{"id":"additional","label":"Additional Metadata","entries":[{"key":"dc:description.abstract","label":"Abstract","values":["An initial study into the use of the large chamber scanning electron microscope (LCSEM) to interrogate the surface microstructure evolution of metallic specimens has been carried out. The LC-SEM located at Western Kentucky University is the largest instrument of its type at any university in the world. As such, unique measurements can be performed due to the size of its chamber and extended view of its optic system. Strain was varied for each individual specimen, and imaged using Secondary Electrons within the gauge length as well as near the grip position. Results will show progression of surface microstructures and nickel content of metallic specimens. Additionally, results will demonstrate the capability of the LC-SEM to carry out these types of measurements. Future measurements will include the incorporation of an in-situ uniaxial load frame for dynamic studies.
"]},{"key":"dc:title","label":"Title","values":["Surface Microstructure Evolution of Metallic Specimens Using the Large Chamber Scanning Electron Microscope"]}]}],"canonical_facts":{"dc:contributor":["Edward Kintzel (Director), Keith Andrew, Ivan Novikov"],"dc:creator":["Egbujor, Grace"],"dc:description.abstract":["An initial study into the use of the large chamber scanning electron microscope (LCSEM) to interrogate the surface microstructure evolution of metallic specimens has been carried out. The LC-SEM located at Western Kentucky University is the largest instrument of its type at any university in the world. As such, unique measurements can be performed due to the size of its chamber and extended view of its optic system. Strain was varied for each individual specimen, and imaged using Secondary Electrons within the gauge length as well as near the grip position. Results will show progression of surface microstructures and nickel content of metallic specimens. Additionally, results will demonstrate the capability of the LC-SEM to carry out these types of measurements. Future measurements will include the incorporation of an in-situ uniaxial load frame for dynamic studies.
"],"dc:identifier":["https://digitalcommons.wku.edu/theses/1473"],"dc:subject":["SEM","Microstructure","Electron","Stainless Steel","Condensed Matter Physics","Physics"],"dc:title":["Surface Microstructure Evolution of Metallic Specimens Using the Large Chamber Scanning Electron Microscope"],"dc:type":["Thesis"],"thesis:degree_discipline":["Department of Physics and Astronomy"],"thesis:degree_name":["Master of Science"]},"updated_at":"2026-07-24T06:08:52Z"}