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University of Illinois at Urbana-Champaign

The Degradation of Spatial Resolution in Thin Foil X-Ray Microchemical Analysis Due to Plural Scattering of Electrons

Abstract

dc:description

A computer-based Monte Carlo simulation of incoherent plural scattering of electrons has been developed in order to estimate the broadening of an electron probe as it propagates through a solid. By applying this approach to modeling the spreading of a fine (50 (ANGSTROM)) probe focused on a thin foil in a scanning transmission electron microscope (STEM), we have estimated the spatial resolution of the compositional analysis obtainable using energy dispersive x-ray spectroscopy (EDS). Specifically, an attempt has been made to determine how the apparent microchemistry of a feature of finer dimensions than the broadened beam differs from the actual composition of the given feature.

Degree

thesis:*
Name thesis:degree_name
Ph.D.
Level thesis:degree_level
Dissertation
Discipline thesis:degree_discipline
Metallurgical Engineering
Grantor
University of Illinois at Urbana-Champaign
Year dc:date
2014

Author and committee

dc:creator, dc:contributor.*
Author dc:creator
  • Twigg, Mark Erickson

Subjects

dc:subject × 1

Identifiers

dc:identifier.*
Identifier
(UMI)AAI8303009
OAI identifier oai:identifier
oai:www.ideals.illinois.edu:2142/71798

Chain of custody

source
Harvested from
University of Illinois - Urbana-Champaign
Base URL
www.ideals.illinois.edu/oai-pmh
Last updated
2026-07-22
Source record
OAI-PMH GetRecord
citation

Twigg, Mark Erickson. The Degradation of Spatial Resolution in Thin Foil X-Ray Microchemical Analysis Due to Plural Scattering of Electrons. Dissertation thesis, University of Illinois at Urbana-Champaign, 2014. http://hdl.handle.net/2142/71798