Global ETD Search
Search theses and dissertations gathered from participating repositories worldwide. Every result links back to the library that holds it. No account is needed.
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Showing 1 to 9 of 9 for “"x-ray powder diffractometry"”.
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The Synthesis of Core-Shell Iron@Gold Nanoparticles and Their Characterization
… TEM (transmission electron microscopy), XRD (X-ray Powder Diffractometry), EDS (Energy disperse X-ray spectroscopy), SQUID (Superconducting Quantum Interference Device), TGA (Thermograviometric analysis), UV-visible absorption spectroscopy and Faraday rotation were employed to characterize the …
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Separation of close isomers by enclathration
… were characterised using thermal analysis and X-ray powder diffraction. The lattice energies of the complexes were calculated to determine their relative stability. The kinetics of desolvation of the picoline and lutidine inclusion compounds were studied, using isothermal and non-isothermal …
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The effect of manganese doping on the superconducting transition temperature and the upper critical field of tin-molybdenum-sulfide
… properties. They were characterized by x-ray powder diffractometry, optical microscopy. electron microscopy, and electron microprobe work. The transition temperature decreased slow1~ with increasing manganese content until x=O.06. It then increased until x=O.10. after which it fell slow1~ …
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Structure-activity relationships in Werner clathrates
… have been elucidated by single crystal x-ray analysis. The difficulty has been found to lie in refining disordered guest molecules. Other techniques employed in the initial characterization of these compounds are Microanalysis, Mass Spectrometry and UV/Visible Spectrophotometry. An …
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Metal phosphates: From syntheses and structures to applications in sorption, catalysis and teeth erosion protection
… were structurally analyzed by single crystal X-ray diffraction. The thermal properties and stability were investigated using thermogravimetry (TGA) together with X-ray powder diffractometry (XRPD) to elucidate the loss of guest molecules and the stability of the host framework. Crystals grown …
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Synthesis and Investigation of Nanomaterials by Homogeneous Nonaqueous Solution Phase Reactions
… electron microscopy), EDS (Energy disperse X-ray spectroscopy), XRD (X-ray powder diffractometry), ICP (inductively-coupled plasma spectrometer), TGA (Thermogravimetric analysis), UV-visible absorption spectroscopy, IR (infrared) spectroscopy and SQUID magnetometry (Superconducting Quantum …
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Nanocarriers for drug targeting and improved bioavailability
… carried out by infrared spectroscopy (FTIR), X-ray powder diffractometry (XRPD), differential scanning calorimetry. Dissolution study of PRX ODT was performed in distilled water (pH 5.5) and was compared with PRX coarse suspension ODT, PRX/poloxamer 188 physical mixture, bulk PRX samples and a …
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Co-crystal screening of poorly water-soluble active pharmaceutical ingredients. Application of hot stage microscopy on curcumin-nicotinamide system and construction of ternary phase diagram of fenbufen-nicotinamide-water co-crystal system.
Curcumin is the major phenolic diarylheptane derivative in Curcuma longa and has been reported to possess pharmacological activities. Unfortunately this compound suffers from poor bioavailability and rapid neutral-alkaline degradation. Co-crystal of curcumin is one option under exploration, …