Effects of powder conditioning on the quality, microstructure and mechanical properties of sintered titanium alloys
type: CreativeWork
description: A small amount of internal lubricant (Stearic acid (SA) or Magnesium stearate (MgSt)) was added to Ti powder for the purpose of improving the compressibility and the green density homogeneity. Lubrication improved the compressibility of Ti powder compacts, especially in the low pressure region (<400MPa), yet at higher pressures, lubricants hindered further improvement. An addition of up to 0.3wt.% SA improved the green density. MgSt showed a better lubrication effect and an addition of up to 0.6wt.% improved the density. The difference in the lubrication effect between SA and MgSt was due to their mixing or blending characteristics. A homogenous mixing of lubricant led to an increased lubricated area and the effectiveness of the lubrication. Lubricants had a strong influence on shape retention, green strength and ejection behaviour of Ti powder compacts. The green density distribution was improved by adding a lubricant. The density profiles were measured experimentally using a coloured layer method. SA gave better results compared with MgSt, with 0.6wt.% of SA considered to be the optimum addition. The mixing or blending characteristics of SA additions accounted for the better improvement in performance. By adding a lubricant, the sintered density distribution in Ti compacts was improved by controlling the pore morphology with respect to their size, aspect ratio and orientation. But 1wt.% SA created many pores ranging in size from 50-100μm, both in the top and bottom regions, and this led to very bad ductility. The consistency in mechanical properties of a sintered Ti Φ40 mm compact was significantly improved by adding 0.6wt.% SA. Such improvement was achieved because of a lower sintering mismatch initiated from a more homogenously distributed green density, both in the horizontal and transverse directions. MgSt was not recommended because of higher oxygen pick-up. Rare earth elements (RE) were added to Ti metal and alloy for the purpose of scavenging oxygen and to …
abstract: A small amount of internal lubricant (Stearic acid (SA) or Magnesium stearate (MgSt)) was added to Ti powder for the purpose of improving the compressibility and the green density homogeneity. Lubrication improved the compressibility of Ti powder compacts, especially in the low pressure region (<400MPa), yet at higher pressures, lubricants hindered further improvement. An addition of up to 0.3wt.% SA improved the green density. MgSt showed a better lubrication effect and an addition of up to 0.6wt.% improved the density. The difference in the lubrication effect between SA and MgSt was due to their mixing or blending characteristics. A homogenous mixing of lubricant led to an increased lubricated area and the effectiveness of the lubrication. Lubricants had a strong influence on shape retention, green strength and ejection behaviour of Ti powder compacts. The green density distribution was improved by adding a lubricant. The density profiles were measured experimentally using a coloured layer method. SA gave better results compared with MgSt, with 0.6wt.% of SA considered to be the optimum addition. The mixing or blending characteristics of SA additions accounted for the better improvement in performance. By adding a lubricant, the sintered density distribution in Ti compacts was improved by controlling the pore morphology with respect to their size, aspect ratio and orientation. But 1wt.% SA created many pores ranging in size from 50-100μm, both in the top and bottom regions, and this led to very bad ductility. The consistency in mechanical properties of a sintered Ti Φ40 mm compact was significantly improved by adding 0.6wt.% SA. Such improvement was achieved because of a lower sintering mismatch initiated from a more homogenously distributed green density, both in the horizontal and transverse directions. MgSt was not recommended because of higher oxygen pick-up. Rare earth elements (RE) were added to Ti metal and alloy for the purpose of scavenging oxygen and to …
author: Lou, Jia
keywords: Power metallurgy, Titanium, Powder conditioning, Microstructure, Mechanical properties
license: https://researchcommons.waikato.ac.nz/bitstreams/1d6d4edb-168f-473a-a5ae-c2ffaf12e611/download
date published: 2015
date modified: 2026-07-24T05:57:18Z
provider: University Waikato
publisher: Networked Digital Library of Theses and Dissertations
type: WebPage
source organization: University of Waikato