{"id":{"repo_id":"birmingham","oai_identifier":"oai:etheses.bham.ac.uk:592"},"canonical_url":"https://search.dev.ndltd.org/etd/birmingham/oai:etheses.bham.ac.uk:592","repository":{"repo_id":"birmingham","name":"University of Birmingham","base_url":"https://etheses.bham.ac.uk/cgi/oai2"},"display":{"title":"Characterisation of anode supported microtubular SOFC process on pure methane reduction and operation","abstract":"The optimisations of reduction and operation of Ni-YSZ anode supported micro tubular cells on pure methane were studied. A major problem of SOFCs is nickel anode performance on methane and higher hydrocarbons. The aim of this work was to study the effect of reduction and operation of anode-supported microtubular SOFCs using methane as both reductant and fuel. The results were compared to those from optimised operation using hydrogen. To measure mechanical strength, the three point bending test was employed. Temperature programmed oxidation (TPO) results were investigated to measure the carbon deposition on the anode in order to assess potential damage to the cermet catalyst. Also field emission scanning electron microscope (FE-SEM) and Energy-Dispersive X-ray spectroscopy EDS results were analysed on the anode surface.","abstract_html":"The optimisations of reduction and operation of Ni-YSZ anode supported micro tubular cells on pure methane were studied. A major problem of SOFCs is nickel anode performance on methane and higher hydrocarbons. The aim of this work was to study the effect of reduction and operation of anode-supported microtubular SOFCs using methane as both reductant and fuel. The results were compared to those from optimised operation using hydrogen. To measure mechanical strength, the three point bending test was employed. Temperature programmed oxidation (TPO) results were investigated to measure the carbon deposition on the anode in order to assess potential damage to the cermet catalyst. Also field emission scanning electron microscope (FE-SEM) and Energy-Dispersive X-ray spectroscopy EDS results were analysed on the anode surface.","abstract_has_math":false,"creators":["Lee, Tae Jung"],"institution":"University of Birmingham","degree_name":"d_ph","degree_level":"d_ph","degree_discipline":null,"degree_department":null,"school":null,"contributors":[],"advisors":[],"committee_chairs":[],"committee_members":[],"year":2010,"date_issued":"2010-07","date_published":"2010-07","updated_at":"2026-07-24T01:11:02Z","subjects":["TP Chemical technology","QD Chemistry"],"languages":[],"rights":[],"rights_urls":[],"identifier_entries":[]},"links":{"outbound_url":null,"outbound_label":null,"outbound_source":null},"metadata_groups":[{"id":"people","label":"People","entries":[{"key":"dc:contributor.sponsor","label":"Sponsor","values":["na"]},{"key":"dc:creator","label":"Author","values":["Lee, Tae Jung"]}]},{"id":"academic_context","label":"Academic Context","entries":[{"key":"dc:date","label":"Dc Date","values":["2010-07"]},{"key":"dc:date.issued","label":"Date","values":["2010-07"]},{"key":"dc:publisher.department","label":"Dc Publisher Department","values":["College of Engineering & Physical Sciences","School of Chemical Engineering"]},{"key":"dc:publisher.institution","label":"Dc Publisher Institution","values":["University of Birmingham"]},{"key":"dc:relation.isreferencedby","label":"Dc Relation Isreferencedby","values":["http://etheses.bham.ac.uk//id/eprint/592/"]},{"key":"dc:type","label":"Dc Type","values":["Thesis"]},{"key":"dc:type.qualificationlevel","label":"Dc Type Qualificationlevel","values":["d_ph"]},{"key":"dc:type.qualificationname","label":"Dc Type Qualificationname","values":["d_ph"]}]},{"id":"subjects_keywords","label":"Subjects and Keywords","entries":[{"key":"dc:subject","label":"Dc Subject","values":["TP Chemical technology","QD Chemistry"]}]},{"id":"identifiers","label":"Identifiers","entries":[{"key":"dc:identifier.uri","label":"Identifier URI","values":["http://etheses.bham.ac.uk//id/eprint/592/1/Lee10PhD.pdf","http://etheses.bham.ac.uk//id/eprint/592/2/Decl_IS_Lee10PhD.pdf"]}]},{"id":"additional","label":"Additional Metadata","entries":[{"key":"dc:description.abstract","label":"Abstract","values":["The optimisations of reduction and operation of Ni-YSZ anode supported micro tubular cells on pure methane were studied. A major problem of SOFCs is nickel anode performance on methane and higher hydrocarbons. The aim of this work was to study the effect of reduction and operation of anode-supported microtubular SOFCs using methane as both reductant and fuel. The results were compared to those from optimised operation using hydrogen. To measure mechanical strength, the three point bending test was employed. Temperature programmed oxidation (TPO) results were investigated to measure the carbon deposition on the anode in order to assess potential damage to the cermet catalyst. Also field emission scanning electron microscope (FE-SEM) and Energy-Dispersive X-ray spectroscopy EDS results were analysed on the anode surface."]},{"key":"dc:format","label":"Dc Format","values":["application/pdf"]},{"key":"dc:title","label":"Title","values":["Characterisation of anode supported microtubular SOFC process on pure methane reduction and operation"]}]}],"canonical_facts":{"dc:contributor.sponsor":["na"],"dc:creator":["Lee, Tae Jung"],"dc:date":["2010-07"],"dc:date.issued":["2010-07"],"dc:description.abstract":["The optimisations of reduction and operation of Ni-YSZ anode supported micro tubular cells on pure methane were studied. A major problem of SOFCs is nickel anode performance on methane and higher hydrocarbons. The aim of this work was to study the effect of reduction and operation of anode-supported microtubular SOFCs using methane as both reductant and fuel. The results were compared to those from optimised operation using hydrogen. To measure mechanical strength, the three point bending test was employed. Temperature programmed oxidation (TPO) results were investigated to measure the carbon deposition on the anode in order to assess potential damage to the cermet catalyst. Also field emission scanning electron microscope (FE-SEM) and Energy-Dispersive X-ray spectroscopy EDS results were analysed on the anode surface."],"dc:format":["application/pdf"],"dc:identifier.uri":["http://etheses.bham.ac.uk//id/eprint/592/1/Lee10PhD.pdf","http://etheses.bham.ac.uk//id/eprint/592/2/Decl_IS_Lee10PhD.pdf"],"dc:publisher.department":["College of Engineering & Physical Sciences","School of Chemical Engineering"],"dc:publisher.institution":["University of Birmingham"],"dc:relation.isreferencedby":["http://etheses.bham.ac.uk//id/eprint/592/"],"dc:subject":["TP Chemical technology","QD Chemistry"],"dc:title":["Characterisation of anode supported microtubular SOFC process on pure methane reduction and operation"],"dc:type":["Thesis"],"dc:type.qualificationlevel":["d_ph"],"dc:type.qualificationname":["d_ph"]},"updated_at":"2026-07-24T01:11:02Z"}