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Showing 1 to 1 of 1 for “"syn SE'"”.
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The development of palladium-catalyzed cross-coupling reactions of allylic silanolate salts with aromatic bromides
… bromides cross-coupled in poor yield because of a secondary isomerization to the 1-propeneyl isomer (or concommitant polymerization). A modified protocol that employs an electron-rich phosphine ligand (SPhos), a lower reaction temperature (40 °C), and a less polar solvent (toluene) delivers …