Global ETD Search
Search theses and dissertations gathered from participating repositories worldwide. Every result links back to the library that holds it. No account is needed.
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Showing 1 to 3 of 3 for “"dipolar aprotic solvent"”.
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Synthesis and characterization of novel macromolecules/networks via side chain modifications of amorphous poly(arylene ethers)
… nucleophilic aromatic substitution with a dipolar aprotic solvent, toluene as the azeotroping agent, and a slight excess of potassium carbonate as the weak base was the preferred methodology. The concentration of amines along the polymer backbone was successfully controlled by varying the …
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Synthesis and characteristics of polyarylene ether sulfones
… substitution using dimethylsulfoxide (DMSO) as a dipolar aprotic solvent and aqueous sodium hydroxide as a base. High molecular weight homopolymers can be synthesized in a short time (1 hour). However, hydrolytic side reactions can limit its scope for the synthesis of block copolymers. An …
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Sustainable P2 design for batch-based specialty chemical manufacture
… on the reduction of n-methyl-2-pyrrilodone (NMP) solvent waste in the manufacture of polyimide and polybenzoxazole precursors. The evaluation includes the environmental and economic assessment of solvent recovery and substitution strategies. A two-step distillation process proved effective in …