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Showing 1 to 1 of 1 for “"Oganic synthesis of 1-Benzthiocin"”.
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Synthesis of 2H-1-Benzthiocin: a Precursor for the Generation of the "4n+2" Pi-electron 1-Benzthiocinide Anion.
… was prepared by LAH reduction of 2-mercaptobenzoic acid (thiosalicylic acid) in 95% yield. Oxidation of it with PCC afforded 2,2'-dithiobenzaldehyde <strong>15</strong> in 52% yield. A selective reduction of disulfide <strong>15</strong> to 2-mercaptobvenzaldehyde …