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Showing 1 to 8 of 8 for “"Dioxanone"”.

  1. Asymmetrische Synthese von Sordidin, 7-epi-Sordidin und von Polyoeinheiten mit quartären Stereozentren

    … banana plants has been achieved. Starting from dioxanone RAMP-hydrazone the desired C-7 epimers were prepared in 39% overall yield as a 1.5: 1 diastereomeric mixture over 14 steps. The epimers could be separated by preparative GC and thus, each of them could be obtained in high diastereomeric …

    aachen Repository record for Asymmetrische Synthese von Sordidin, 7-epi-Sordidin und von Polyoeinheiten mit quartären Stereozentren (opens in a new tab)

  2. Asymmetric synthesis of (+)-altholactone, a styryllactone from various goniothalamus species

    … the well-established 1,3-diol building block, dioxanone (2,2-dimethyl-1,3-dioxan-5-one) 4, is described. This approach is based on establishment of the chiral centres by applying a RAMP-directed alkylation (ee > 98 %), an asymmetric aldol reaction (ee, de > 98 %) and a selective reduction (de > …

    aachen Repository record for Asymmetric synthesis of (+)-altholactone, a styryllactone from various goniothalamus species (opens in a new tab)

  3. Zur asymmetrischen Synthese von C-Azanucleosiden und 2-Amino-1,3-diolen

    … was synthesized starting from the Dioxanone-RAMP-hydrazone in a seven-step procedure. The desired product was obtained in 47% overall yield, with excellent diastereo- and enatiomeric excess (de, ee>=96%).

    aachen Repository record for Zur asymmetrischen Synthese von C-Azanucleosiden und 2-Amino-1,3-diolen (opens in a new tab)

  4. 1,3-Aminoalkohole als Bausteine in der asymmetrischen Synthese von Azetidinen, Azetidincarbonsäuren und Piperidin-3-olen

    … in a diastereoselective alkylation of the dioxanone SAMP-hydrazone. The obtained aminoketon was cyclised by reductive amination, yielding an acetal protected piperidin-3-ol. Different protecting group strategies were examined in order to increase the moderate yields and …

    aachen Repository record for 1,3-Aminoalkohole als Bausteine in der asymmetrischen Synthese von Azetidinen, Azetidincarbonsäuren und Piperidin-3-olen (opens in a new tab)

  5. Amorphe bioabbaubare Poly(esterurethan)netzwerksysteme mit Formgedächtniseigenschaften

    … and diglycolide, E-caprolactone or p-dioxanone. Covalent networks are formed by polyaddition of precursors and a diisocyanate acting as coupling agent. The glass transition temperature Tg of the networks corresponds to the transition temperature Ttrans of the shape-memory effect. The …

    aachen Repository record for Amorphe bioabbaubare Poly(esterurethan)netzwerksysteme mit Formgedächtniseigenschaften (opens in a new tab)

  6. Novel sulfur containing electrophiles in asymmetric organocatalysis

    … works well with acid-sensitive compounds such as dioxanone. We also evaluated the reactivity of various phenylthiomethyl amines towards protonation. We claim that aromatic are a stable class of compounds, which do not undergo acid-catalyzed cleavage of free amine to furnish a reactive carbocation. …

    aachen Repository record for Novel sulfur containing electrophiles in asymmetric organocatalysis (opens in a new tab)

  7. Asymmetrische Synthese von 2-Methyl-substituierten 1,3-Diolen

    Nature employs dihydroxyacetonephosphate (DHAP) as a C3-building block for carbohydrate synthesis via enzyme catalyzed aldol reactions. Accordingly many groups focussed on broadening the scope of that enzyme catalyzed reaction. On the other hand a chiral, synthetic DHAP equivalent would not only be …

    aachen Repository record for Asymmetrische Synthese von 2-Methyl-substituierten 1,3-Diolen (opens in a new tab)